The accumulation of soil organic carbon (SOC) and total nitrogen (TN) is easily accomplished by returning crop straw, which strongly affects the formation and pore structure of aggregates, especially in black soil. We returned maize straw at different rates (6,000, 9,000, 12,000 and 15,000 kg ha(-1)) for nine years to investigate its influence on the SOC and TN contents in the SOC fractions of aggregates by combining size and density fractionation. Their subsequent influences on pore morphology and size distribution characteristics were examined using X-ray micro-computed tomography scanning (mu CT). The results showed that returning straw significantly increased the contents of C and N in the SOC fractions of aggregates, especially at the return rates of 12,000 and 15,000 kg ha(-1), which in turn promoted aggregate formation and stability, and ultimately amended pore structure. The pore size>100 mu m, porosity (>2 mu m), and morphological characteristics (anisotropy, circularity, connectivity and fractal dimension) significantly increased, but the total number of pores significantly decreased (P<0.05). Our results indicated that the amendment of the pore morphology and size distribution of soil aggregates was primarily controlled by the higher contents of C and N in the density fractions of aggregates, rather than in the aggregate sizes. Furthermore, this pore network reconfiguration favored the storage of C and N simultaneously. The findings of this study offer valuable new insights into the relationships between C and N storage and the pore characteristics in soil aggregates under straw return.

This paper investigates the effects of particle morphology (PM) and particle size distribution (PSD) on the micro-macro mechanical behaviours of granular soils through a novel X-ray micro-computed tomography (mu CT)-based discrete element method (DEM) technique. This technique contains the grain-scale property extraction by the X-ray mu CT, DEM parameter calibration by the one-to-one mapping technique, and the massive derivative DEM simulations. In total, 25 DEM samples were generated with a consideration of six PSDs and four PMs. The effects of PSD and PM on the micro-macro mechanical behaviours were carefully investigated, and the coupled effects were highlighted. It is found that (a) PM plays a significant role in the micro-macro mechanical responses of granular soils under triaxial shear; (b) the PSD uniformity can enhance the particle morphology effect in dictating the peak deviatoric stress, maximum volumetric strain, contact-based coordination number, fabric evolution, and shear band formation, while showing limited influences in the maximum dilation angle and particle-based coordination number; (c) with the same PSD uniformity and PM degree, the mean particle volume shows minimal effects on the macro-micro mechanical behaviours of granular soils as well as the particle morphology effects.

Fujian River sand (FJS) is a complex mixture of minerals and rock fragments shaped by the dynamic geological history of Fujian province, China. The macro-micro mechanical responses of FJS under triaxial shear were carefully investigated through the X-ray tomography-based in situ triaxial test. By utilising the particle tracking strategy with the signature of histograms of orientation, both intact and crushed FJS particles can be successfully recognised and tracked at different stages of axial strain. It is found that (a) smaller particles are more likely to crush than larger ones, and the crushed particles have more irregular particle shapes than the original set of particles; (b) the coordination number, fabric anisotropy, 3D rose map, and particle displacement are found to highly correlate to the phase transition point from volumetric contraction to dilation; (c) the sample deformation is found to be uniform at the early stage, and then it starts to spread from the boundaries to the inner part and finally develops into an inclined shear band; (d) locations of particle breakage within the granular assemblage show an overall sporadic and irregular pattern throughout the shearing process, which is not strongly correlated with the shear band that has developed, even at large strains.