This study examined the physical, mechanical, tribological, and corrosion properties of copper metal matrix composites reinforced with zirconium diboride (ZrB 2). Cu-xZrB 2 composites (x = 0.5, 10, 15, 20 wt.%) were produced by the ball-milling process and spark plasma sintering (SPS). Introducing ZrB 2 particles into copper matrix composites significantly improves their mechanical and tribological properties while deteriorating their density, porosity, and corrosion properties. It was shown that the relative densities of the composites gradually decreased from 96% to 90%, with an increase in the ZrB 2 content to 20 wt.%. Likewise, hardness, compressive strength, and wear resistance improved with increasing ZrB 2 content in the copper matrix. Corrosion resistance tests in a 0.05 M sulfuric acid environment showed a disproportionate decrease in the resistance of this composite with an increase in the concentration of the ceramic phase compared to other environments. Abstract This study examined the physical, mechanical, tribological, and corrosion properties of copper metal matrix composites reinforced with zirconium diboride (ZrB 2). Cu-xZrB 2 composites (x = 0.5, 10, 15, 20 wt.%) were produced by the ball-milling process and spark plasma sintering (SPS). Introducing ZrB 2 particles into copper matrix composites significantly improves their mechanical and tribological properties while deteriorating their density, porosity, and corrosion properties. It was shown that the relative densities of the composites gradually decreased from 96% to 90%, with an increase in the ZrB 2 content to 20 wt.%. Likewise, hardness, compressive strength, and wear resistance improved with increasing ZrB 2 content in the copper matrix. Corrosion resistance tests in a 0.05 M sulfuric acid environment showed a disproportionate decrease in the resistance of this composite with an increase in the concentration of the ceramic phase compared to other environments. Keywords: copper matrix composites; ZrB2; powder metallurgy; mechanical properties; wear resistance; corrosion resistance